12423 NE Whitaker Way
Portland, OR 97230
503-254-1794

Job Number:         19-009812

Report Number:   19-009812-00

Report Date:         08/22/2019

ORELAP#:             OR100028

Purchase Order:

Received:               08/15/19 10:54

This report cannot be used for ODA, OHA or OLCC compliance requirements.

Product Identity: Tincture 1000mg Vanilla

Laboratory ID: 19-009812-0002

Client/Metric ID:

Sample Date:

Summary

Potency:

Analyte per 30g
Result
Limit
Units
LOQ
CBC per 30g†
8.85
mg/30g
1.00
CBD per 30g†
1010
mg/30g
1.00
CBDV per 30g†
5.01
mg/30g
1.00
CBG per 30g†
1.61
mg/30g
1.00
CBN per 30g
2.12
mg/30g
1.00
Δ9-THC per 30g
1.91
mg/30g
1.00
CBD – Total per 30g
1010 mg/30g
THC – Total per 30g
< 1.91 mg/30g

(Report in milligrams per serving)

Terpenes:

Analyte
Percent by weight
Analyte
Percentage by weight
a-Bisabolol†
0.0563
(-)-Guaiol†
0.0334
Total Terpenes†
0.0897

Customer:                       Nirvana CBD

Product identity:            Tincture 1000mg Vanilla

Client/Metric ID:

Sample Date:

Laboratory ID:                  19-009812-0002

Relinquished by:               Patrick Mulcahy

Temp:                                 26.6° C

Serving Size #1:              30g

Sample Results

Potency per 30g                                                                                           Batch: 1907558

Analyte
Result
Limits
Units
LOQ
Analyze
Method
Notes
CBC per 30g†
8.85
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBC-A per 30g†
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBC-Total per 30g†
8.85
mg/30g
1.88
08/22/19
J AOAC 2015 V98-6
CBD per 30g
1010
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBD-A per 30g
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBD-Total per 30g
1010
mg/30g
1.88
08/22/19
J AOAC 2015 V98-6
CBDV per 30g†
5.01
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBDV-A per 30g†
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBDV-Total per 30g†
5.01
mg/30g
1.87
08/22/19
J AOAC 2015 V98-6
CBG per 30g†
1.61
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBG-A per 30g†
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBG-Total per 30g†
< LOQ
mg/30g
1.88
08/22/19
J AOAC 2015 V98-6
CBL per 30g†
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
CBN per 30g
2.12
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
Δ8-THC per 30g†
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
Δ9-THC per 30g
1.91
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
THC-A per 30g
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
THC-Total per 30g
1.91
mg/30g
1.88
08/22/19
J AOAC 2015 V98-6
THCV per 30g†
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
THCV-A per 30g†
< LOQ
mg/30g
1.000
08/22/19
J AOAC 2015 V98-6
THCV-Total per 30g†
< LOQ
mg/30g
1.87
08/22/19
J AOAC 2015 V98-6

Terpenes

Method J AOAC 2015 V98-6

Unit %

Batch 1907400

Analyze 08/16/19 01:53 PM

Analyte
Result
LOQ
Note
Analyze
Result
LOQ
Notes
a-Bisabolol†
0.0563
0.020
(-)-Guaiol†
0.0334
0.020
ß-Caryophyllene†
< LOQ
0.020
(-)-a-Terpineol†
< LOQ
0.020
(-)-caryophyllene oxide†
< LOQ
0.020
(-)-Isopulegol†
< LOQ
0.020
(-)-ß-Pinene†
< LOQ
0.020
(+)-Borneol†
< LOQ
0.020
(+)-Cedrol†
< LOQ
0.020
(+)-fenchol†
< LOQ
0.020
(+)-Pulegone†
< LOQ
0.020
(±)-Camphor†
< LOQ
0.020
(±)-cis-Nerolidol†
< LOQ
0.020
(±)-fenchone†
< LOQ
0.020
(±)-trans-Nerolidol†
< LOQ
0.020
(R)-(+)-Limonene†
< LOQ
0.020
a-cedrene†
< LOQ
0.020
a-phellandrene†
< LOQ
0.020
a-pinene†
< LOQ
0.020
a-Terpinene†
< LOQ
0.020
Camphene†
< LOQ
0.020
cis-ß-Ocimene†
< LOQ
0.020
d-3-Carene†
< LOQ
0.020
Eucalyptol†
< LOQ
0.006
farnesene†
< LOQ
0.020
gamma-Terpinene†
< LOQ
0.020
Geraniol†
< LOQ
0.020
Geranyl acetate†
< LOQ
0.020
Humulene†
< LOQ
0.020
Isoborneol†
< LOQ
0.020
Linalool†
< LOQ
0.020
Menthol†
< LOQ
0.020
nerol†
< LOQ
0.020
p-Cymene†
< LOQ
0.020
Sabinene†
< LOQ
0.020
Sabinene hydrate†
< LOQ
0.020
ß-Myrcene†
< LOQ
0.020
Terpinolene†
< LOQ
0.020
trans-ß-Ocimene†
< LOQ
0.013
valencene†
< LOQ
0.020
Total Terpenes
0.0897

Abbreviations

Limits: Action Levels per OAR-333-007-0400, OAR-333-007-0210, OAR-333-007-0220

Limits(s) of Quantitation (LOQ): The minimum levels, concetrations, or quantitites of a target variable (e.g., target analyte) that can be reported with a specified degree of confidence.

† = Analyte not NELAP accredited.

Units of Measure

g= Gram

mg/30g = Milligram per 30g

% = Percentage of sample

% wt = μg/g divided by 10,000

Laboratory Terpene Quality Control Results

EPA 5035

Batch ID: 306

Method Bank

Laboratory Control Sample

Analyte
Result
Blank
Notes
Result
LCS Spike
Units
LCS % Rec
% Limits
Notes
a-pinene
ND
< 200
421
500
μg/g
84.3
70 – 130
Camphene
ND
< 200
427
500
μg/g
85.3
70 – 130
Sabinene
ND
< 200
408
500
μg/g
81.7
70 – 130
b-Pinene
ND
< 200
421
500
μg/g
84.2
70 – 130
b-Myrcene
ND
< 200
429
500
μg/g
85.8
70 – 130
a-phelllandrene
ND
< 200
456
500
μg/g
91.2
70 – 130
d-3-Carene
ND
< 200
459
500
μg/g
91.8
70 – 130
a-Terpinene
ND
< 200
441
500
μg/g
88.1
70 – 130
p-Cymene
ND
< 200
433
500
μg/g
86.6
70 – 130
D-Limonene
ND
< 200
444
500
μg/g
88.7
70 – 130
Eucalyptol
ND
< 200
429
500
μg/g
85.7
70 – 130
b-cis-Ocimene
ND
< 66.7
138
167
μg/g
82.8
70 – 130
b-trans-Ocimene
ND
< 133
303
333
μg/g
90.9
70 – 130
g-Terpinene
ND
< 200
433
500
μg/g
86.7
70 – 130
Sabinene_Hydrate
ND
< 200
380
500
μg/g
76.0
70 – 130
Terpinolene
ND
< 200
409
500
μg/g
81.8
70 – 130
D-Fenchone
ND
< 200
427
500
μg/g
85.3
70 – 130
Linalool
ND
< 200
414
500
μg/g
82.8
70 – 130
Fenchol
ND
< 200
427
500
μg/g
85.4
70 – 130
Camphor
ND
< 200
398
500
μg/g
79.6
70 – 130
Isopulego
ND
< 200
416
500
μg/g
83.2
70 – 130
Isoborneol
ND
< 200
436
500
μg/g
87.1
70 – 130
Borneol
ND
< 200
419
500
μg/g
83.8
70 – 130
DL-Menthol
ND
< 200
436
500
μg/g
87.2
70 – 130
Terpineol
ND
< 200
359
500
μg/g
71.8
70 – 130
Nerol
ND
< 200
450
500
μg/g
90.0
70 – 130
Pulegone
ND
< 200
436
500
μg/g
87.2
70 – 130
Gereniol
ND
< 200
389
500
μg/g
77.9
70 – 130
Geranyl_Acetate
ND
< 200
425
500
μg/g
85.1
70 – 130
a-Cedrene
ND
< 200
418
500
μg/g
83.7
70 – 130
b-Caryophyllene
ND
< 200
483
500
μg/g
96.6
70 – 130
a-Humulene
ND
< 200
436
500
μg/g
87.2
70 – 130
Valenene
ND
< 200
437
500
μg/g
87.5
70 – 130
cis-Nerolidol
ND
< 200
455
500
μg/g
91.0
70 – 130
a-Farnesene
ND
< 200
572
500
μg/g
114.3
70 – 130
trans-Nerolidol
ND
< 200
405
500
μg/g
81.0
70 – 130
Caryophyllene_Oxide
ND
< 200
398
500
μg/g
79.5
70 – 130
Guaiol
ND
< 200
402
500
μg/g
80.4
70 – 130
Cedrol
ND
< 200
408
500
μg/g
81.6
70 – 130
a-Bisabolol
ND
< 200
417
500
μg/g
83.3
70 – 130

Sample / Sample Duplicate

Sample ID: 19-009812-0001

Analyte
Result
Org. Result
LOQ
Units
RPD, %
Sample Duplicate
% Limits
Notes
a-pinene
ND
ND
200
μg/g
0
< 20
80 – 120
Camphene
ND
ND
200
μg/g
0
< 20
80 – 120
Sabinene
ND
ND
200
μg/g
0
< 20
80 – 120
b-Pinene
ND
ND
200
μg/g
0
< 20
80 – 120
b-Myrcene
ND
ND
200
μg/g
0
< 20
80 – 120
a-phelllandrene
ND
ND
200
μg/g
0
< 20
80 – 120
d-3-Carene
ND
ND
200
μg/g
0
< 20
80 – 120
a-Terpinene
ND
ND
200
μg/g
0
< 20
80 – 120
p-Cymene
ND
ND
200
μg/g
0
< 20
80 – 120
D-Limonene
ND
ND
200
μg/g
0
< 20
80 – 120
Eucalyptol
ND
ND
200
μg/g
0
< 20
80 – 120
b-cis-Ocimene
ND
ND
66.7
μg/g
0
< 20
80 – 120
b-trans-Ocimene
ND
ND
133
μg/g
0
< 20
80 – 120
g-Terpinene
ND
ND
200
μg/g
0
< 20
80 – 120
Sabinene_Hydrate
ND
ND
200
μg/g
0
< 20
80 – 120
Terpinolene
ND
ND
200
μg/g
0
< 20
80 – 120
D-Fenchone
ND
ND
200
μg/g
0
< 20
80 – 120
Linalool
ND
ND
200
μg/g
0
< 20
80 – 120
Fenchol
ND
ND
200
μg/g
0
< 20
80 – 120
Camphor
ND
ND
200
μg/g
0
< 20
80 – 120
Isopulego
ND
ND
200
μg/g
0
< 20
80 – 120
Isoborneol
ND
ND
200
μg/g
0
< 20
80 – 120
Borneol
ND
ND
200
μg/g
0
< 20
80 – 120
DL-Menthol
ND
ND
200
μg/g
0
< 20
80 – 120
Terpineol
ND
ND
200
μg/g
0
< 20
80 – 120
Nerol
ND
ND
200
μg/g
0
< 20
80 – 120
Pulegone
ND
ND
200
μg/g
0
< 20
80 – 120
Gereniol
ND
ND
200
μg/g
0
< 20
80 – 120
Geranyl_Acetate
ND
ND
200
μg/g
0
< 20
80 – 120
a-Cedrene
ND
ND
200
μg/g
0
< 20
80 – 120
b-Caryophyllene
ND
ND
200
μg/g
0
< 20
80 – 120
a-Humulene
ND
ND
200
μg/g
0
< 20
80 – 120
Valenene
ND
ND
200
μg/g
0
< 20
80 – 120
cis-Nerolidol
ND
ND
200
μg/g
0
< 20
80 – 120
a-Farnesene
ND
ND
200
μg/g
0
< 20
80 – 120
trans-Nerolidol
ND
ND
200
μg/g
0
< 20
80 – 120
Caryophyllene_Oxide
ND
ND
200
μg/g
0
< 20
80 – 120
Guaiol
ND
ND
200
μg/g
0
< 20
80 – 120
Cedrol
ND
ND
200
μg/g
0
< 20
80 – 120
a-Bisabolol
ND
ND
200
μg/g
0
< 20
80 – 120

Laboratory Quality Control Result

J AOAC 2015 V98-6

Batch ID: 1907558

Laboratory Control Sample

Analyte
Result
Spike
Units
%Rec
Limits
Evaluation
Notes
CBDV-A
0.00889
0.01
%
88.9
85 – 115
Acceptable
CBDV
0.00891
0.01
%
89.1
85 – 115
Acceptable
CBD-A
0.00897
0.01
%
89.7
85 – 115
Acceptable
CBG-A
0.00881
0.01
%
88.1
85 – 115
Acceptable
CBG
0.00893
0.01
%
89.3
85 – 115
Acceptable
CBD
0.00929
0.01
%
92.9
85 – 115
Acceptable
THCV
0.00877
0.01
%
87.7
85 – 115
Acceptable
THCVA
0.00920
0.01
%
92.0
85 – 115
Acceptable
CBN
0.00927
0.01
%
92.7
85 – 115
Acceptable
THC
0.00904
0.01
%
90.4
85 – 115
Acceptable
D8THC
0.00861
0.01
%
86.1
85 – 115
Acceptable
CBL
0.00882
0.01
%
88.2
85 – 115
Acceptable
CBC
0.00914
0.01
%
91.4
85 – 115
Acceptable
THCA
0.00960
0.01
%
96.0
85 – 115
Acceptable
CBCA
0.00852
0.01
%
85.2
85 – 115
Acceptable

Method Bank

Analyte
Result
LOQ
Units
Limits
Evaluation
Notes
CBDV-A
ND
0.003
%
< 0.003
Acceptable
CBDV
ND
0.003
%
< 0.003
Acceptable
CBD-A
ND
0.003
%
< 0.003
Acceptable
CBG-A
ND
0.003
%
< 0.003
Acceptable
CBG
ND
0.003
%
< 0.003
Acceptable
CBD
ND
0.003
%
< 0.003
Acceptable
THCV
ND
0.003
%
< 0.003
Acceptable
THCVA
ND
0.003
%
< 0.003
Acceptable
CBN
ND
0.003
%
< 0.003
Acceptable
THC
ND
0.003
%
< 0.003
Acceptable
D8THC
ND
0.003
%
< 0.003
Acceptable
CBL
ND
0.003
%
< 0.003
Acceptable
CBC
ND
0.003
%
< 0.003
Acceptable
THCA
ND
0.003
%
< 0.003
Acceptable
CBCA
ND
0.003
%
< 0.003
Acceptable

Abbreviations

ND – None Detected at above MRL

RPD – Relative Percent Difference

LOQ – Limit of Quantitation

 

Units of Measure:

% – Percent

 

J AOAC 2015 V98-6

Sample Duplicate

Batch ID: 1907558

Sample ID: 19-009812-0002

Analyte
Result
Org. Result
LOQ
Units
RPD
Limits
Evaluation
Notes
CBDV-A
ND
ND
0.003
%
0
< 20
Acceptable
CBDV
0.0167
0.0167
0.003
%
0
< 20
Acceptable
CBD-A
ND
ND
0.003
%
0
< 20
Acceptable
CBG-A
ND
ND
0.003
%
0
< 20
Acceptable
CBG
0.00542
0.00538
0.003
%
0.741
< 20
Acceptable
CBD
3.38
3.35
0.003
%
0.892
< 20
Acceptable
THCV
ND
ND
0.003
%
0
< 20
Acceptable
THCVA
ND
ND
0.003
%
0
< 20
Acceptable
CBN
0.00705
0.00706
0.003
%
0.142
< 20
Acceptable
THC
0.00638
0.00637
0.003
%
0.157
< 20
Acceptable
D8THC
ND
ND
0.003
%
0
< 20
Acceptable
CBL
ND
ND
0.003
%
0
< 20
Acceptable
CBC
0.0296
0.0296
0.003
%
0
< 20
Acceptable
THCA
ND
ND
0.003
%
0
< 20
Acceptable
CBCA
ND
ND
0.003
%
0
< 20
Acceptable

Abbreviations

ND – None Detected at above MRL

RPD – Relative Percent Difference

LOQ – Limit of Quantitation

 

Units of Measure:

% – Percent

 

Explanation of QC Comments:

Code
Explanation
Q
Matrix interferences affecting spike or surrogate recoveries.
Q1
Quality control result biased high. Only non-detect samples reported.
Q2
Quality control outside QC limits. Data considered estimate.
Q3
Sample concentration greater than four times the amount spiked.
Q4
Non-homogenous sample matrix, affecting RPD result and/or % recoveries.
Q5
Spike results above calibration curve.
Q6
Quality control outside QC limits. Data acceptable based on remaining QC.
R
Relative percent difference (RPD) outside control limit.
R1
RPD non-calculable, as sample or duplicate results are less than five times the LOQ.
R2
Sample replicates RPD non-calculable, as only one replicate is within the analytical range.
LOQ1
Quantitation level raised due to low sample volume and/or dilution.
LOQ2
Quantitaion level raised due to matrix interference.
B
Analyte detected in method blank, but not in associated samples.
B1
The sample concentration is greater than 5 times the blank concentration.
B2
The sample concentration is less than 5 times the blank concentration.

Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unless otherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless prior arrangements have been made.

 

Testing in accordance with: OAR-333-007-0430

12423 NE Whitaker Way
Portland, OR 97230
503-254-1794

Streamline Vape Co.

Garden Grove, CA 92841
patrick@nirvanacbd.com
(714) 343 – 3409
Lic. #CBD

Certificate of Analysis

Powered by Confident Cannabis

Sample: 1905DBL0343.5139
METRC Sample:

Strain: Vanilla Flavor
Ordered: 05/30/2019; Sampled: 05/30/2019;Completed:06/03/2019

Nirvana CBD Tincture 1000MG Vanilla Flavor

Ingestible, Tincture

Cannabinoid
CBC
CBCa
CBD
CBDa
CBDV
CBDVa
CBG
CBGa
CBL
CBN
Δ8-THC
Δ9-THC
THCa
THCV
THCVa

Cannabinoids

<LOQ

∆9-THC + ∆8-THC

1,034.727 mg/unit

CBD

1,041.203 mg/unit

Total Cannabinoids

NT

Moisture

1 Unit = Nirvana CBD Tincture 1000MG Vanilla Flavor; Density = 0.9526 g/mL, 28.5768g

Cannabinoid Profile

Analyzed by 300.18 UHPLC/PDA

Cannabinoid
Mass
Mass
LOQ
mg/unit
mg/g
mg/unit
CBC
< LOQ
< LOQ
1.736
CBCa
< LOQ
< LOQ
1.736
CBD
1034.727
36.209
1.736
CBDa
< LOQ
< LOQ
1.736
CBDV
6.476
0.227
1.736
CBDVa
< LOQ
< LOQ
1.736
CBG
< LOQ
< LOQ
1.736
CBGa
< LOQ
< LOQ
1.736
CBL
< LOQ
< LOQ
1.736
CBN
< LOQ
< LOQ
1.736
Δ8-THC
< LOQ
< LOQ
1.736
Δ9-THC
< LOQ
< LOQ
1.736
THCa
< LOQ
< LOQ
1.736
THCV
< LOQ
< LOQ
1.736
THCVa
< LOQ
< LOQ
1.736
TOTAL THC
ND
ND
TOTAL CBD
1,034.727
36.209
TOTAL
1041.203
36.435

Terpenes

Analyzed by 300.13 GC/FID and GC/MS

Compound
LOQ
Mass
Mass
Relative Concentration
mg/unit
mg/unit
mg/g
α-Bisabolol
2.596
7.177
0.251
Caryophyllene Oxide
2.596
4.320
0.151
Guaiol
2.596
4.287
0.150
β-Caryophyllene
2.596
3.855
0.135
trans-Nerolidol
0.909
1.678
0.059
α -Humulene
2.596
< LOQ
< LOQ
α-Pinene
2.596
< LOQ
< LOQ
α-Terpinene
2.596
< LOQ
< LOQ
β-Myrcene
2.596
< LOQ
< LOQ
β-Pinene
2.596
< LOQ
< LOQ
Camphene
2.596
< LOQ
< LOQ
cis-Nerolidol
1.687
< LOQ
< LOQ
cis-Ocimene
1.687
< LOQ
< LOQ
δ-3-Carene
2.596
< LOQ
< LOQ
δ-Limonene
2.596
< LOQ
< LOQ
Eucalyptol
2.596
< LOQ
< LOQ
γ-Terpinene
2.596
< LOQ
< LOQ
Isopulegol
2.596
< LOQ
< LOQ
Linalool
2.596
< LOQ
< LOQ
p-Cymene
2.596
< LOQ
< LOQ
Terpinolene
2.596
< LOQ
< LOQ
trans-Ocimene
0.909
< LOQ
< LOQ

21.316 mg/unit

Total Terpenes

CBD Tincture Chamomile

The reported result is based on a sample weight with the applicable moisture content for that sample. LOQ = Limit of Quantitation. Pesticide LOQ = Instrument Limit of Quantitation, NA = Not Analyzed. ND = Not Detected. NR = Not Reported. NT = Not Tested. PGR = Plant Growth Regulator. Unless otherwise stated all quality control samples performed within specifications established by the Laboratory. This product has been tested by DB Labs, LLC (MME# 61887736101164525768) using valid testing methodologies and a quality system as required by Nevada state law. Edibles are picked up prior to final packaging unless otherwise stated. Values reported relate only to the product tested. The uncertainty of measurement associated with the measurement result reported in this certificate is available from the organization upon request. DB Labs makes no claims as to the efficacy, safety or other risks associated with any detected or non-detected levels of any compounds reported herein. This Certi􀃗cate shall not be reproduced except in full, without the written approval of DB Labs.

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