Nirvana CBD Tincture Grapefruit Flavor 500mg

12423 NE Whitaker Way
Portland, OR 97230
503-254-1794

Job Number: 19-009812

Report Number: 19-009812-00

Report Date: 08/22/2019

ORELAP#: OR100028

Purchase Order:

Received: 08/15/19 10:54

This report cannot be used for ODA, OHA or OLCC compliance requirements.

Product Identity: Tincture 500mg Grapefruit

Laboratory ID: 19-009812-0012

Client/Metric ID:

Sample Date:

Summary

Potency:

Analyte per 30g	Result	Units	LOQ

CBC per 30g†	1.50	mg/30g	1.00
CBD per 30g†	579	mg/30g	1.00
CBDV per 30g†	3.36	mg/30g	1.00
CBL per 30g†	1.12	mg/30g	1.00


CBD – Total per 30g	579 mg/30g
THC – Total per 30g	< 1.878 mg/30g

(Report in milligrams per serving)

Terpenes:

Analyte	Percent by weight	Analyte	Percentage by weight

(R)-(+)-Limonene†	9.86	ß-Myrcene†	0.158
a-Bisabolol†	0.0508	a-pinene†	0.0482
ß-Caryophyllene†	0.0396	(-)-Guaiol†	0.0322
Total Terpenes†	10.2

Customer: Nirvana CBD

Product identity: Tincture 500mg Grapefruit

Client/Metric ID:

Sample Date:

Laboratory ID: 19-009812-0012

Relinquished by: Patrick Mulcahy

Temp: 26.6° C

Serving Size #1: 30g

Sample Results

Potency per 30g Batch: 1907558

Analyte	Result	Units	LOQ	Analyze	Method

CBC per 30g†	1.50	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBC-A per 30g†	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBC-Total per 30g†	< LOQ	mg/30g	1.88	08/22/19	J AOAC 2015 V98-6
CBD per 30g	579	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBD-A per 30g	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBD-Total per 30g	579	mg/30g	1.88	08/22/19	J AOAC 2015 V98-6
CBDV per 30g†	3.36	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBDV-A per 30g†	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBDV-Total per 30g†	3.36	mg/30g	1.87	08/22/19	J AOAC 2015 V98-6
CBG per 30g†	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBG-A per 30g†	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBG-Total per 30g†	< LOQ	mg/30g	1.88	08/22/19	J AOAC 2015 V98-6
CBL per 30g†	1.12	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
CBN per 30g	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
Δ8-THC per 30g†	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
Δ9-THC per 30g	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
THC-A per 30g	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
THC-Total per 30g	< LOQ	mg/30g	1.88	08/22/19	J AOAC 2015 V98-6
THCV per 30g†	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
THCV-A per 30g†	< LOQ	mg/30g	1.000	08/22/19	J AOAC 2015 V98-6
THCV-Total per 30g†	< LOQ	mg/30g	1.87	08/22/19	J AOAC 2015 V98-6

Terpenes

Method J AOAC 2015 V98-6

Unit %

Batch 1907400

Analyze 08/16/19 01:53 PM

Analyte	Result	LOQ	Analyze	Result	LOQ

(R)-(+)-Limonene†	9.86	0.020	ß-Myrcene†	0.158	0.020
a-Bisabolol†	0.0508	0.020	a-pinene†	0.0482	0.020
ß-Caryophyllene†	0.0396	0.020	Sabinene†	< LOQ	0.020
(-)-a-Terpineol†	< LOQ	0.020	(-)-caryophyllene oxide†	< LOQ	0.020
(-)-Guaiol†	< LOQ	0.020	(-)-Isopulegol†	< LOQ	0.020
(-)-ß-Pinene†	< LOQ	0.020	(+)-Borneol†	< LOQ	0.020
(+)-Cedrol†	< LOQ	0.020	(+)-fenchol†	< LOQ	0.020
(+)-Pulegone†	< LOQ	0.020	(±)-Camphor†	< LOQ	0.020
(±)-cis-Nerolidol†	< LOQ	0.020	(±)-fenchone†	< LOQ	0.020
(±)-trans-Nerolidol†	< LOQ	0.020	a-cedrene†	< LOQ	0.020
a-phellandrene†	< LOQ	0.020	a-Terpinene†	< LOQ	0.020
Camphene†	< LOQ	0.020	cis-ß-Ocimene†	< LOQ	0.006
d-3-Carene†	< LOQ	0.020	Eucalyptol†	< LOQ	0.020
farnesene†	< LOQ	0.020	gamma-Terpinene†	< LOQ	0.020
Geraniol†	< LOQ	0.020	Geranyl acetate†	< LOQ	0.020
Humulene†	< LOQ	0.020	Isoborneol†	< LOQ	0.020
Linalool†	< LOQ	0.020	Menthol†	< LOQ	0.020
nerol†	< LOQ	0.020	p-Cymene†	< LOQ	0.020
Sabinene hydrate†	< LOQ	0.020	Terpinolene†	< LOQ	0.020
trans-ß-Ocimene†	< LOQ	0.013	valencene†	< LOQ	0.020
Total Terpenes	10.2

Abbreviations

Limits: Action Levels per OAR-333-007-0400, OAR-333-007-0210, OAR-333-007-0220

Limits(s) of Quantitation (LOQ): The minimum levels, concetrations, or quantitites of a target variable (e.g., target analyte) that can be reported with a specified degree of confidence.

† = Analyte not NELAP accredited.

Units of Measure

g= Gram

mg/30g = Milligram per 30g

% = Percentage of sample

% wt = μg/g divided by 10,000

EPA 5035

Batch ID: 306

Method Bank

Laboratory Control Sample

Analyte	Result	Blank	Result	LCS Spike	Units	LCS % Rec	% Limits

a-pinene	ND	< 200	421	500	μg/g	84.3	70 – 130
Camphene	ND	< 200	427	500	μg/g	85.3	70 – 130
Sabinene	ND	< 200	408	500	μg/g	81.7	70 – 130
b-Pinene	ND	< 200	421	500	μg/g	84.2	70 – 130
b-Myrcene	ND	< 200	429	500	μg/g	85.8	70 – 130
a-phelllandrene	ND	< 200	456	500	μg/g	91.2	70 – 130
d-3-Carene	ND	< 200	459	500	μg/g	91.8	70 – 130
a-Terpinene	ND	< 200	441	500	μg/g	88.1	70 – 130
p-Cymene	ND	< 200	433	500	μg/g	86.6	70 – 130
D-Limonene	ND	< 200	444	500	μg/g	88.7	70 – 130
Eucalyptol	ND	< 200	429	500	μg/g	85.7	70 – 130
b-cis-Ocimene	ND	< 66.7	138	167	μg/g	82.8	70 – 130
b-trans-Ocimene	ND	< 133	303	333	μg/g	90.9	70 – 130
g-Terpinene	ND	< 200	433	500	μg/g	86.7	70 – 130
Sabinene_Hydrate	ND	< 200	380	500	μg/g	76.0	70 – 130
Terpinolene	ND	< 200	409	500	μg/g	81.8	70 – 130
D-Fenchone	ND	< 200	427	500	μg/g	85.3	70 – 130
Linalool	ND	< 200	414	500	μg/g	82.8	70 – 130
Fenchol	ND	< 200	427	500	μg/g	85.4	70 – 130
Camphor	ND	< 200	398	500	μg/g	79.6	70 – 130
Isopulego	ND	< 200	416	500	μg/g	83.2	70 – 130
Isoborneol	ND	< 200	436	500	μg/g	87.1	70 – 130
Borneol	ND	< 200	419	500	μg/g	83.8	70 – 130
DL-Menthol	ND	< 200	436	500	μg/g	87.2	70 – 130
Terpineol	ND	< 200	359	500	μg/g	71.8	70 – 130
Nerol	ND	< 200	450	500	μg/g	90.0	70 – 130
Pulegone	ND	< 200	436	500	μg/g	87.2	70 – 130
Gereniol	ND	< 200	389	500	μg/g	77.9	70 – 130
Geranyl_Acetate	ND	< 200	425	500	μg/g	85.1	70 – 130
a-Cedrene	ND	< 200	418	500	μg/g	83.7	70 – 130
b-Caryophyllene	ND	< 200	483	500	μg/g	96.6	70 – 130
a-Humulene	ND	< 200	436	500	μg/g	87.2	70 – 130
Valenene	ND	< 200	437	500	μg/g	87.5	70 – 130
cis-Nerolidol	ND	< 200	455	500	μg/g	91.0	70 – 130
a-Farnesene	ND	< 200	572	500	μg/g	114.3	70 – 130
trans-Nerolidol	ND	< 200	405	500	μg/g	81.0	70 – 130
Caryophyllene_Oxide	ND	< 200	398	500	μg/g	79.5	70 – 130
Guaiol	ND	< 200	402	500	μg/g	80.4	70 – 130
Cedrol	ND	< 200	408	500	μg/g	81.6	70 – 130
a-Bisabolol	ND	< 200	417	500	μg/g	83.3	70 – 130

Sample / Sample Duplicate

Sample ID: 19-009812-0001

Analyte	Result	Org. Result	LOQ	Units	RPD, %	Sample Duplicate	% Limits

a-pinene	ND	ND	200	μg/g	0	< 20	80 – 120
Camphene	ND	ND	200	μg/g	0	< 20	80 – 120
Sabinene	ND	ND	200	μg/g	0	< 20	80 – 120
b-Pinene	ND	ND	200	μg/g	0	< 20	80 – 120
b-Myrcene	ND	ND	200	μg/g	0	< 20	80 – 120
a-phelllandrene	ND	ND	200	μg/g	0	< 20	80 – 120
d-3-Carene	ND	ND	200	μg/g	0	< 20	80 – 120
a-Terpinene	ND	ND	200	μg/g	0	< 20	80 – 120
p-Cymene	ND	ND	200	μg/g	0	< 20	80 – 120
D-Limonene	ND	ND	200	μg/g	0	< 20	80 – 120
Eucalyptol	ND	ND	200	μg/g	0	< 20	80 – 120
b-cis-Ocimene	ND	ND	66.7	μg/g	0	< 20	80 – 120
b-trans-Ocimene	ND	ND	133	μg/g	0	< 20	80 – 120
g-Terpinene	ND	ND	200	μg/g	0	< 20	80 – 120
Sabinene_Hydrate	ND	ND	200	μg/g	0	< 20	80 – 120
Terpinolene	ND	ND	200	μg/g	0	< 20	80 – 120
D-Fenchone	ND	ND	200	μg/g	0	< 20	80 – 120
Linalool	ND	ND	200	μg/g	0	< 20	80 – 120
Fenchol	ND	ND	200	μg/g	0	< 20	80 – 120
Camphor	ND	ND	200	μg/g	0	< 20	80 – 120
Isopulego	ND	ND	200	μg/g	0	< 20	80 – 120
Isoborneol	ND	ND	200	μg/g	0	< 20	80 – 120
Borneol	ND	ND	200	μg/g	0	< 20	80 – 120
DL-Menthol	ND	ND	200	μg/g	0	< 20	80 – 120
Terpineol	ND	ND	200	μg/g	0	< 20	80 – 120
Nerol	ND	ND	200	μg/g	0	< 20	80 – 120
Pulegone	ND	ND	200	μg/g	0	< 20	80 – 120
Gereniol	ND	ND	200	μg/g	0	< 20	80 – 120
Geranyl_Acetate	ND	ND	200	μg/g	0	< 20	80 – 120
a-Cedrene	ND	ND	200	μg/g	0	< 20	80 – 120
b-Caryophyllene	ND	ND	200	μg/g	0	< 20	80 – 120
a-Humulene	ND	ND	200	μg/g	0	< 20	80 – 120
Valenene	ND	ND	200	μg/g	0	< 20	80 – 120
cis-Nerolidol	ND	ND	200	μg/g	0	< 20	80 – 120
a-Farnesene	ND	ND	200	μg/g	0	< 20	80 – 120
trans-Nerolidol	ND	ND	200	μg/g	0	< 20	80 – 120
Caryophyllene_Oxide	ND	ND	200	μg/g	0	< 20	80 – 120
Guaiol	ND	ND	200	μg/g	0	< 20	80 – 120
Cedrol	ND	ND	200	μg/g	0	< 20	80 – 120
a-Bisabolol	ND	ND	200	μg/g	0	< 20	80 – 120

J AOAC 2015 V98-6

Batch ID: 1907558

Laboratory Control Sample

Analyte	Result	Spike	Units	%Rec	Limits	Evaluation

CBDV-A	0.00889	0.01	%	88.9	85 – 115	Acceptable
CBDV	0.00891	0.01	%	89.1	85 – 115	Acceptable
CBD-A	0.00897	0.01	%	89.7	85 – 115	Acceptable
CBG-A	0.00881	0.01	%	88.1	85 – 115	Acceptable
CBG	0.00893	0.01	%	89.3	85 – 115	Acceptable
CBD	0.00929	0.01	%	92.9	85 – 115	Acceptable
THCV	0.00877	0.01	%	87.7	85 – 115	Acceptable
THCVA	0.00920	0.01	%	92.0	85 – 115	Acceptable
CBN	0.00927	0.01	%	92.7	85 – 115	Acceptable
THC	0.00904	0.01	%	90.4	85 – 115	Acceptable
D8THC	0.00861	0.01	%	86.1	85 – 115	Acceptable
CBL	0.00882	0.01	%	88.2	85 – 115	Acceptable
CBC	0.00914	0.01	%	91.4	85 – 115	Acceptable
THCA	0.00960	0.01	%	96.0	85 – 115	Acceptable
CBCA	0.00852	0.01	%	85.2	85 – 115	Acceptable

Method Bank

Analyte	Result	LOQ	Units	Limits	Evaluation

CBDV-A	ND	0.003	%	< 0.003	Acceptable
CBDV	ND	0.003	%	< 0.003	Acceptable
CBD-A	ND	0.003	%	< 0.003	Acceptable
CBG-A	ND	0.003	%	< 0.003	Acceptable
CBG	ND	0.003	%	< 0.003	Acceptable
CBD	ND	0.003	%	< 0.003	Acceptable
THCV	ND	0.003	%	< 0.003	Acceptable
THCVA	ND	0.003	%	< 0.003	Acceptable
CBN	ND	0.003	%	< 0.003	Acceptable
THC	ND	0.003	%	< 0.003	Acceptable
D8THC	ND	0.003	%	< 0.003	Acceptable
CBL	ND	0.003	%	< 0.003	Acceptable
CBC	ND	0.003	%	< 0.003	Acceptable
THCA	ND	0.003	%	< 0.003	Acceptable
CBCA	ND	0.003	%	< 0.003	Acceptable

Abbreviations

ND – None Detected at above MRL

RPD – Relative Percent Difference

LOQ – Limit of Quantitation

Units of Measure:

% – Percent

J AOAC 2015 V98-6

Sample Duplicate

Batch ID: 1907558

Sample ID: 19-009812-0002

Analyte	Result	Org. Result	LOQ	Units	RPD	Limits	Evaluation

CBDV-A	ND	ND	0.003	%	0	< 20	Acceptable
CBDV	0.0167	0.0167	0.003	%	0	< 20	Acceptable
CBD-A	ND	ND	0.003	%	0	< 20	Acceptable
CBG-A	ND	ND	0.003	%	0	< 20	Acceptable
CBG	0.00542	0.00538	0.003	%	0.741	< 20	Acceptable
CBD	3.38	3.35	0.003	%	0.892	< 20	Acceptable
THCV	ND	ND	0.003	%	0	< 20	Acceptable
THCVA	ND	ND	0.003	%	0	< 20	Acceptable
CBN	0.00705	0.00706	0.003	%	0.142	< 20	Acceptable
THC	0.00638	0.00637	0.003	%	0.157	< 20	Acceptable
D8THC	ND	ND	0.003	%	0	< 20	Acceptable
CBL	ND	ND	0.003	%	0	< 20	Acceptable
CBC	0.0296	0.0296	0.003	%	0	< 20	Acceptable
THCA	ND	ND	0.003	%	0	< 20	Acceptable
CBCA	ND	ND	0.003	%	0	< 20	Acceptable

Abbreviations

ND – None Detected at above MRL

RPD – Relative Percent Difference

LOQ – Limit of Quantitation

Units of Measure:

% – Percent

Explanation of QC Comments:

Code	Explanation

Q	Matrix interferences affecting spike or surrogate recoveries.
Q1	Quality control result biased high. Only non-detect samples reported.
Q2	Quality control outside QC limits. Data considered estimate.
Q3	Sample concentration greater than four times the amount spiked.
Q4	Non-homogenous sample matrix, affecting RPD result and/or % recoveries.
Q5	Spike results above calibration curve.
Q6	Quality control outside QC limits. Data acceptable based on remaining QC.
R	Relative percent difference (RPD) outside control limit.
R1	RPD non-calculable, as sample or duplicate results are less than five times the LOQ.
R2	Sample replicates RPD non-calculable, as only one replicate is within the analytical range.
LOQ1	Quantitation level raised due to low sample volume and/or dilution.
LOQ2	Quantitaion level raised due to matrix interference.
B	Analyte detected in method blank, but not in associated samples.
B1	The sample concentration is greater than 5 times the blank concentration.
B2	The sample concentration is less than 5 times the blank concentration.

Test results relate only to the parameters tested and to the samples as received by the laboratory. Test results meet all requirements of NELAP and the Pixis quality assurance plan unless otherwise noted. This report shall not be reproduced, except in full, without the written consent of this laboratory. Samples will be kept a maximum of 15 days from the report date unless prior arrangements have been made.

Testing in accordance with: OAR-333-007-0430

12423 NE Whitaker Way
Portland, OR 97230
503-254-1794

This report cannot be used for ODA, OHA or OLCC compliance requirements.

Product Identity: Tincture 500mg Grapefruit

Laboratory ID: 19-009812-0012

Client/Metric ID:

Sample Date:

Summary

Potency:

Terpenes:

Sample Results

Terpenes

Method J AOAC 2015 V98-6

Unit %

Batch 1907400

Analyze 08/16/19 01:53 PM

EPA 5035

Batch ID: 306

Method Bank

Laboratory Control Sample

Sample / Sample Duplicate

Sample ID: 19-009812-0001

J AOAC 2015 V98-6

Batch ID: 1907558

Laboratory Control Sample

Method Bank

J AOAC 2015 V98-6

Sample Duplicate

Batch ID: 1907558

Sample ID: 19-009812-0002

Explanation of QC Comments:

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